This material stands up to pump upsets such as cavitation and dry running.
by Dr. Robert Cook (Lancer Systems)
December 31, 2014

Minimizing pump downtime directly affects the bottom line. Sealless mag-drive and canned-motor pumps, commonplace in the petrochemical and power industries, enhance reliability and reduce emissions and leakage compared with more traditional sealed pumps. The choice between sealless and sealed pumps often involves savings in both time and money. Making the right choice can also affect the overall health and reliability of operations.

Bearing Material Limitations

Sealless pumps use sleeve bearings typically machined from carbon graphite or sintered silicon carbide (SiC). The hardness of these materials allows them to withstand wear during the pumping of aggregate solid media. However, the limited dry-running performance of carbon graphite relegates its use to systems with minimal loads and constant lubrication.

SiC bearings have excellent tribological performance, wear resistance and chemical resistance but can suffer from catastrophic brittle fractures.

The bearings have difficulty absorbing the shocks and vibrations encountered during pump upset conditions. Both carbon graphite and SiC are vulnerable to thermal and mechanical shock, leading to fracture and, ultimately, bearing failure.

Carbon graphite and SiC bearings operate well during steady-state pump operating conditions but are prone to catastrophic failure within modest pump upset conditions. During a catastrophic bearing failure, shards of high-hardness ceramic can lead to total pump failure. The failure results in significant downtime and financial burden.

High-Performance Ceramic Compound

A ceramic matrix composite (CMC) was developed to address the shortcomings of monolithic bearing materials. The high-performance compound is engineered to have similar corrosion protection and wear characteristics compared with monolithic SiC ceramics. The composite displayed greater fracture resistance, tunable surface hardness, and thermal and electrical conductivity control.

The CMC is composed of a fiber-reinforced material with either a silicon oxycarbide or silicon carbide matrix. Surface, bulk and tribological properties can be tuned through fillers and fiber surface treatments, tailoring the engineered material to specific applications. For example, the composite’s low thermal expansion coefficient can be controlled by modifying bulk crystallinity, internal fiber type and fiber architecture. In a bearing application, the modified engineering material can be used in direct contact with stainless steel shafts, mitigating the need for metallic tolerance rings to create an interference fit.

Engineers at the JX Nippon Chemical Texas Inc. in Pasadena, Texas, worked with providers to perform testing on CMC bearings reinforced with carbon fiber. The company wanted to reduce downtime from regular replacement of OEM monolithic carbon graphite bearings. The bearings regularly failed because of vibration fractures during cavitation and/or dry-run conditions.

JX Nippon’s engineers believed the CMC’s thermal and mechanical fracture resistances would increase bearing resiliency during pump upset conditions.

Four Stages of Testing

An internal-circulation Teikoku USA Inc. G-362 canned-motor pump with a Stellite 1 coated rotating shaft served as the test equipment (see Figure 1). The process fluid was an ambient aromatic hydrocarbon with a viscosity of 3.0 centipoise (cP) and a discharge pressure of 100 pounds per square inch (psig). The test’s CMC bearing assemblies were supplied per the manufacturing drawing and consisted of a machined CMC core heat-pressed and pinned in a steel carrier (see Figure 2).

Canned-motor pump with ceramic matrix composite bearingsFigure 1. Canned-motor pump with ceramic matrix composite bearings in orange (Images and graphics courtesy of Lancer Systems)
Ceramic matrix composite bearing and pinned steel carrier assemblyFigure 2. Ceramic matrix composite bearing and pinned steel carrier assembly

The CMC bearing set, defined as both the front and rear location carrier assemblies, were subjected to the following test in four stages. The first stage ran the pump with the CMC bearings for six hours to ensure no immediate issues were evident. The second stage ran the pump under normal operating conditions for 30 days. The process fluid was recirculated to ensure the pump ran for at least 40 hours per week. The pump was disassembled, inspected, measured and then rebuilt after the 30-day test. The total pump run time was 171.75 hours.

During the third stage, the pump underwent controlled cavitation for eight cycles of five minutes each. The cavitation cycles were controlled and induced by inline valves approximately 5 feet from both the suction and discharge. Pump cavitation was induced at a moderate level and then increased. The pump was disassembled, inspected, measured and then rebuilt after the cavitation test.

In the fourth and final stage, the pump was initially run dry for a short duration. The pump was then started under normal operating conditions, followed by process fluid being blown out of the pump. The process fluid wet the bearings without flooding them. After the dry run, the pump was primed and brought back to normal operating conditions simulating thermal shock conditions. The dry run lasted approximately eight minutes; stabilization took approximately 14 minutes.